Synthesis and characterization of [1,14C] N-methylneodecanamide

A. Charig; K. Kinscherf; B. Gargiullo; S. Roman; T. F. Connors; C. Unkefer; I. T. Horvath

doi:10.1002/(sici)1099-1344(200002)43:2<177::aid-jlcr304>3.3.co;2-r

Synthesis and characterization of [1,¹⁴C] N-methylneodecanamide

A. Charig, K. Kinscherf, B. Gargiullo, S. Roman, T. F. Connors, C. Unkefer, I. T. Horvath

Research output: Journal Publications and Reviews › RGC 21 - Publication in refereed journal › peer-review

2 Citations (Scopus)

Abstract

[1-¹⁴C] N-methylneodecanamide (MNDA), a potent insect-repellent, was synthesized from [1-¹²C] neodecanoic acid (NDA) by an exchange variant of the Koch reaction, followed by conversion to the acyl halide and methylamination. The product had all the characteristics of authentic commercial MNDA, and the radiocarbon was distributed among the isomers in the same proportions as the isomers were among the mass.

Original language	English
Pages (from-to)	177-184
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	43
Issue number	2
DOIs	https://doi.org/10.1002/(sici)1099-1344(200002)43:2<177::aid-jlcr304>3.3.co;2-r
Publication status	Published - 2000
Externally published	Yes

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title = "Synthesis and characterization of [1,14C] N-methylneodecanamide",

abstract = "[1-14C] N-methylneodecanamide (MNDA), a potent insect-repellent, was synthesized from [1-12C] neodecanoic acid (NDA) by an exchange variant of the Koch reaction, followed by conversion to the acyl halide and methylamination. The product had all the characteristics of authentic commercial MNDA, and the radiocarbon was distributed among the isomers in the same proportions as the isomers were among the mass.",

author = "A. Charig and K. Kinscherf and B. Gargiullo and S. Roman and Connors, {T. F.} and C. Unkefer and Horvath, {I. T.}",

year = "2000",

doi = "10.1002/(sici)1099-1344(200002)43:2<177::aid-jlcr304>3.3.co;2-r",

language = "English",

volume = "43",

pages = "177--184",

journal = "Journal of Labelled Compounds and Radiopharmaceuticals",

issn = "0362-4803",

publisher = "John Wiley & Sons",

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TY - JOUR

T1 - Synthesis and characterization of [1,14C] N-methylneodecanamide

AU - Charig, A.

AU - Kinscherf, K.

AU - Gargiullo, B.

AU - Roman, S.

AU - Connors, T. F.

AU - Unkefer, C.

AU - Horvath, I. T.

PY - 2000

Y1 - 2000

N2 - [1-14C] N-methylneodecanamide (MNDA), a potent insect-repellent, was synthesized from [1-12C] neodecanoic acid (NDA) by an exchange variant of the Koch reaction, followed by conversion to the acyl halide and methylamination. The product had all the characteristics of authentic commercial MNDA, and the radiocarbon was distributed among the isomers in the same proportions as the isomers were among the mass.

AB - [1-14C] N-methylneodecanamide (MNDA), a potent insect-repellent, was synthesized from [1-12C] neodecanoic acid (NDA) by an exchange variant of the Koch reaction, followed by conversion to the acyl halide and methylamination. The product had all the characteristics of authentic commercial MNDA, and the radiocarbon was distributed among the isomers in the same proportions as the isomers were among the mass.

UR - http://www.scopus.com/inward/record.url?scp=0033984951&partnerID=8YFLogxK

UR - https://www.scopus.com/record/pubmetrics.uri?eid=2-s2.0-0033984951&origin=recordpage

U2 - 10.1002/(sici)1099-1344(200002)43:2<177::aid-jlcr304>3.3.co;2-r

DO - 10.1002/(sici)1099-1344(200002)43:2<177::aid-jlcr304>3.3.co;2-r

M3 - RGC 21 - Publication in refereed journal

SN - 0362-4803

VL - 43

SP - 177

EP - 184

JO - Journal of Labelled Compounds and Radiopharmaceuticals

JF - Journal of Labelled Compounds and Radiopharmaceuticals

IS - 2

ER -