Structure and mechanical property evaluation of Cr-Ti-B-N coatings

Li-Wei Ho, Jyh-Wei Lee*, Hsien-Wei Chen, Yu-Chen Chan, Jenq-Gong Duh

*Corresponding author for this work

Research output: Journal Publications and ReviewsRGC 21 - Publication in refereed journalpeer-review

16 Citations (Scopus)

Abstract

In this study, five Cr-Ti-B-N thin films with different B/(Cr + Ti) ratios ranging from 0.1 to 0.69 were fabricated on silicon substrates and AISI420 stainless steel disks by pulsed DC magnetron sputtering using the Cr and TiB2 targets. It was found that the B content had strong influences on the structures and mechanical properties of Cr-Ti-B-N coatings. When the boron content reached 17 at.%, the microstructure changed from the nanocolumnar structure to a nanocomposite structure with nanograins around 4 nm in diameter embedded in the amorphous matrix. As compared with Cr-B-N coating, the solution hardening effect was found to result from the addition of Ti element. The average surface roughness, hardness and elastic modulus of Cr-Ti-B-N film decreased with increasing B content due to the amorphous BN phase. No chipping failures were found adjacent to the scratch track or indentation craters of each coating. In this study, the 37.3 Cr-2.3 Ti-4.0 B-56.0 N (in at.%) coating provided an optimal combination of hardness, wear resistance and adhesion.
Original languageEnglish
Pages (from-to)380-385
JournalThin Solid Films
Volume544
Online published5 Mar 2013
DOIs
Publication statusPublished - 1 Oct 2013
Externally publishedYes

Funding

The authors gratefully acknowledge the financial support of the National Science Council, Taiwan through contract no. NSC 100-2221-E-131-008-MY3 .

Research Keywords

  • Adhesion test
  • Cr-Ti-B-N thin film
  • Daimler Benz Rockwell-C (HRC-DB)
  • Nanocomposite coating
  • Pulsed DC magnetron sputtering
  • Scratch test

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