Solid state crystal growth of BiScO 3-Pb(Mg 1/3Nb 2/3) O 3-PbTiO 3

Jong Bong Lim; Shujun Zhang; Ho-Yong Lee; Thomas R. Shrout

doi:10.1007/s10832-012-9745-0

Solid state crystal growth of BiScO ₃-Pb(Mg _1/3Nb _2/3) O ₃-PbTiO ₃

Jong Bong Lim
, Shujun Zhang
, Ho-Yong Lee
, Thomas R. Shrout

Research output: Journal Publications and Reviews › RGC 21 - Publication in refereed journal › peer-review

11 Citations (Scopus)

Abstract

Single crystals 0.26BiScO ₃-0.25Pb(Mg _1/3Nb _2/3) O ₃-0.49PbTiO ₃ [BSPMNT] have been grown for the first time by the solid-state crystal growth (SSCG) method. A 〈110〉 oriented Ba(Zr,Ti)O ₃ crystal seed was embedded in a matrix of BSPMNT compact which was annealed at high temperatures to induce the single crystal growth. Various fluxes, including Bi ₂O ₃, LiBiO ₂, PbO/LiBiO ₂, and PbO/Bi ₂O ₃, were used and their effects on the microstructure of the annealed compacts and the single crystal growth behavior were investigated. In the annealed samples with PbO/Bi ₂O ₃ flux, a considerable single crystal growth occurred at 1050 °C (with thickness on the order of 500-1000 μm), without the formation of abnormally large grains in the matrix. The results were explained in terms of the effect of various fluxes, based on the grain growth theory. © Springer Science+Business Media, LLC 2012.

Original language	English
Pages (from-to)	139-143
Journal	Journal of Electroceramics
Volume	29
Issue number	2
DOIs	https://doi.org/10.1007/s10832-012-9745-0
Publication status	Published - Oct 2012
Externally published	Yes

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Publication details (e.g. title, author(s), publication statuses and dates) are captured on an “AS IS” and “AS AVAILABLE” basis at the time of record harvesting from the data source. Suggestions for further amendments or supplementary information can be sent to [email protected].

Research Keywords

Grain growth
Interface
Single crystal

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@article{cbbe8a8cb2c144bcbadd4b1f7d1fc7ca,

title = "Solid state crystal growth of BiScO 3-Pb(Mg 1/3Nb 2/3) O 3-PbTiO 3",

abstract = "Single crystals 0.26BiScO 3-0.25Pb(Mg 1/3Nb 2/3) O 3-0.49PbTiO 3 [BSPMNT] have been grown for the first time by the solid-state crystal growth (SSCG) method. A 〈110〉 oriented Ba(Zr,Ti)O 3 crystal seed was embedded in a matrix of BSPMNT compact which was annealed at high temperatures to induce the single crystal growth. Various fluxes, including Bi 2O 3, LiBiO 2, PbO/LiBiO 2, and PbO/Bi 2O 3, were used and their effects on the microstructure of the annealed compacts and the single crystal growth behavior were investigated. In the annealed samples with PbO/Bi 2O 3 flux, a considerable single crystal growth occurred at 1050 °C (with thickness on the order of 500-1000 μm), without the formation of abnormally large grains in the matrix. The results were explained in terms of the effect of various fluxes, based on the grain growth theory. {\textcopyright} Springer Science+Business Media, LLC 2012.",

keywords = "Grain growth, Interface, Single crystal",

author = "Lim, \{Jong Bong\} and Shujun Zhang and Ho-Yong Lee and Shrout, \{Thomas R.\}",

note = "Publication details (e.g. title, author(s), publication statuses and dates) are captured on an “AS IS” and “AS AVAILABLE” basis at the time of record harvesting from the data source. Suggestions for further amendments or supplementary information can be sent to [email protected].",

year = "2012",

month = oct,

doi = "10.1007/s10832-012-9745-0",

language = "English",

volume = "29",

pages = "139--143",

journal = "Journal of Electroceramics",

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TY - JOUR

T1 - Solid state crystal growth of BiScO 3-Pb(Mg 1/3Nb 2/3) O 3-PbTiO 3

AU - Lim, Jong Bong

AU - Zhang, Shujun

AU - Lee, Ho-Yong

AU - Shrout, Thomas R.

N1 - Publication details (e.g. title, author(s), publication statuses and dates) are captured on an “AS IS” and “AS AVAILABLE” basis at the time of record harvesting from the data source. Suggestions for further amendments or supplementary information can be sent to [email protected].

PY - 2012/10

Y1 - 2012/10

N2 - Single crystals 0.26BiScO 3-0.25Pb(Mg 1/3Nb 2/3) O 3-0.49PbTiO 3 [BSPMNT] have been grown for the first time by the solid-state crystal growth (SSCG) method. A 〈110〉 oriented Ba(Zr,Ti)O 3 crystal seed was embedded in a matrix of BSPMNT compact which was annealed at high temperatures to induce the single crystal growth. Various fluxes, including Bi 2O 3, LiBiO 2, PbO/LiBiO 2, and PbO/Bi 2O 3, were used and their effects on the microstructure of the annealed compacts and the single crystal growth behavior were investigated. In the annealed samples with PbO/Bi 2O 3 flux, a considerable single crystal growth occurred at 1050 °C (with thickness on the order of 500-1000 μm), without the formation of abnormally large grains in the matrix. The results were explained in terms of the effect of various fluxes, based on the grain growth theory. © Springer Science+Business Media, LLC 2012.

AB - Single crystals 0.26BiScO 3-0.25Pb(Mg 1/3Nb 2/3) O 3-0.49PbTiO 3 [BSPMNT] have been grown for the first time by the solid-state crystal growth (SSCG) method. A 〈110〉 oriented Ba(Zr,Ti)O 3 crystal seed was embedded in a matrix of BSPMNT compact which was annealed at high temperatures to induce the single crystal growth. Various fluxes, including Bi 2O 3, LiBiO 2, PbO/LiBiO 2, and PbO/Bi 2O 3, were used and their effects on the microstructure of the annealed compacts and the single crystal growth behavior were investigated. In the annealed samples with PbO/Bi 2O 3 flux, a considerable single crystal growth occurred at 1050 °C (with thickness on the order of 500-1000 μm), without the formation of abnormally large grains in the matrix. The results were explained in terms of the effect of various fluxes, based on the grain growth theory. © Springer Science+Business Media, LLC 2012.

KW - Grain growth

KW - Interface

KW - Single crystal

UR - https://www.scopus.com/pages/publications/84868574898

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U2 - 10.1007/s10832-012-9745-0

DO - 10.1007/s10832-012-9745-0

M3 - RGC 21 - Publication in refereed journal

SN - 1385-3449

VL - 29

SP - 139

EP - 143

JO - Journal of Electroceramics

JF - Journal of Electroceramics

IS - 2

ER -