Abstract
Sol-gel process has been frequently employed for preparation of silica/polyimide composite films. In this article, a novel sol-gel route is introduced to prepare silica (SiO2)/polyimide (PI) (PS2 system) composite films and to enhance the compatibility between the polyimide and silica. The transmittance, mechanical properties, thermal stability, and morphology of the PS2 composites are studied and compared with the PS1 films prepared by the traditional sol-gel route. The results show that the transmittance, mechanical properties and thermal stability of the PS2 composites are significantly improved especially at high silica contents when compared with those of their counterparts prepared by the traditional sol-gel route. This is explained in terms of the silica particle size and dispersion in the two composites. In addition, the effect of silica particle size on the thermal expansion of silica/PI films is also examined. © 2007 Elsevier Ltd. All rights reserved.
| Original language | English |
|---|---|
| Pages (from-to) | 2408-2416 |
| Journal | Composites Science and Technology |
| Volume | 67 |
| Issue number | 11-12 |
| DOIs | |
| Publication status | Published - Sept 2007 |
| Externally published | Yes |
Bibliographical note
Publication details (e.g. title, author(s), publication statuses and dates) are captured on an “AS IS” and “AS AVAILABLE” basis at the time of record harvesting from the data source. Suggestions for further amendments or supplementary information can be sent to [email protected].Research Keywords
- Composites
- Mechanical properties
- Sol-gel
- Thermal expansion
- Thermal stability
- Transmittance
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