Effects of nitrogen implantation on low cycle fatigue behavior of ferritic Fe-24Cr-4Al stainless alloy

The effects of nitrogen implantation on cyclic deformation response, near-surface dislocation substructure, surface slip band formation, crack initiation, and fatigue life under low cycle fatigue of the ferritic Fe-24Cr-4Al stainless alloy were investigated. Implantation was carried out at an energy of 65 keV and at a fluence of 2 × 10¹⁷ ions/cm². Nitrogen implantation resulted in a substantial cyclic hardening in the alloy. Homogeneous planar dislocation arrangements were formed in the near-surface region of implanted specimens after fatigue, while dislocation loop debris and patches were developed in the un-implanted specimens. Moreover, formation of persistent slip bands (PSBs) was greatly suppressed in the surface of the implanted specimens. Nitrogen implantation also resulted in an alteration of the crack initiation mode from the grain boundary to the surface penetration of the PSBs nucleated below the surface layer. Fatigue life improvements after nitrogen implantation could only be obtained when the PSBs were not only suppressed but also homogenized in the implanted surface layer.