Abstract
The dependence of the width of void-denuded zones (VDZs) on grain boundary (GB) characters was investigated in Cu irradiated with He ions at elevated temperature. Dislocation loops and voids formed near GBs during irradiation were characterized by transmission electron microscopy, and GB misorientations and normal planes were determined by electron back-scatter diffraction. The VDZ widths at Σ3〈1 1 0〉 tilt GBs ranged from 0 to 24 nm and increased with the GB plane inclination angle. For non-Σ3 GBs, VDZ widths ranged from 40 to 70 nm and generally increased with misorientation angle. Nevertheless, there is considerable scatter about this general trend, indicating that the remaining crystallographic parameters also play a role in determining the sink efficiencies of these GBs. In addition, the VDZ widths at two sides of a GB show different values for certain asymmetrical GBs. Voids were also observed within GB planes and their density and radius also appeared to depend on GB character. We conclude that GB sink efficiencies depend on the overall GB character, including both misorientation and GB plane orientation. © 2012 Published by Elsevier Ltd. on behalf of Acta Materialia Inc.
| Original language | English |
|---|---|
| Pages (from-to) | 6341-6351 |
| Journal | Acta Materialia |
| Volume | 60 |
| Issue number | 18 |
| DOIs | |
| Publication status | Published - Oct 2012 |
| Externally published | Yes |
Bibliographical note
Publication details (e.g. title, author(s), publication statuses and dates) are captured on an “AS IS” and “AS AVAILABLE” basis at the time of record harvesting from the data source. Suggestions for further amendments or supplementary information can be sent to <a href="mailto:[email protected]">[email protected]</a>.Funding
This work is sponsored by the US Department of Energy, Office of Science, Office of Basic Energy Sciences, Energy Frontier Research Center (EFRC) under Award No. 2008LANL 1026. W.Z.H. acknowledges discussion with Dr. H.Q. Li and assistance from Dr. A. Perez-Bergquist with twin-jet polishing.
Research Keywords
- Grain boundary
- Grain boundary plane
- Misorientation
- Sink efficiency
- Void-denuded zone
Policy Impact
- Cited in Policy Documents
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